HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66727315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 66727467 | HCID 66727467 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66727315 | HCID 66727315 | — |
Reaction Steps
To a solution of 2-methyl-propane-2-sulfinic acid [(S)-1-(3-bromo-isoxazol-5-yl)-propyl]-amide (17.5 mg, 0.0566 mmol) in MeOH (1 mL) was added a 4 M solution of HCl in dioxane (0.70 mL, 0.28 mmol) dropwise. After 2.5 hours, the mixture was concentrated in vacuo to afford the title compound which was used with out purification. MS m/z 188.24 (M-53), 190.20 (M+2-53).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338610B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-0396d21d129f481facac42301a2f53fb |
| Source note | uspto-grants-2012_12 |