Ethylamine → HCID 68909733, compound

Participants

Reaction Steps

The product of Example 10B and ethylamine were processed as in Examples 29A and Example 29B to afford the title compound. 1H NMR (300 MHz, CDCl3) δ ppm 1.18 (s, 1H), 1.21 (s, 6H), 1.26 (t, J=7.3 Hz, 3H), 1.32 (s, 6H), 2.77-2.83 (m, 2H), 3.41-3.55 (m, 2H), 3.98 (t, J=5.3 Hz, 2H), 4.71 (t, J=1.7 Hz, 2H), 5.70-5.82 (m, 1H), 12.02 (s, 1H); MS (DCI/NH3) m/z 352 (M+H)+; anal. calculated for C18H26N2O3S: C, 61.69; H, 7.48; N, 7.99. Found: C, 61.58; H, 7.39; N, 7.94.

Provenance & Evidence