HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 68743533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Ethyl 2-(hexanoylamino)-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate | HCID 1752437 | — |
| Product | HCID 68743533 | HCID 68743533 | — |
Reaction Steps
The product of Example 33 and dimethylamine were processed as in Examples 29A and 29B to afford the title compound. 1H NMR (300 MHz, CDCl3) δ ppm 0.88-0.96 (m, 4H), 1.29-1.41 (m, 4H), 1.54-1.72 (m, 3H), 1.73-1.91 (m, 3H), 2.33-2.42 (m, 4H), 2.63-2.71 (m, 2H), 2.92 (s, 3H), 3.05 (s, 3H); MS (DCI/NH3) m/z 323 (M+H)+; anal. calculated for C17H26N2O2S.0.75C8H17NO.0.3H2O: C, 63.46; H, 9.11; N, 8.85. Found: C, 63.15; H, 9.46; N, 8.66.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338623B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-010ea9e9ee624ccbac2360fa1e3e23e1 |
| Source note | uspto-grants-2012_12 |