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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2198270Generated: October 30, 2026

Ammonia → HCID 68908356, compound

https://huagongshe.com/reaction/2198270

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantAzetidine hydrochlorideHCID 12308726—
ReactantHCID 68910107HCID 68910107—
ProductHCID 68908356HCID 68908356—

Reaction Steps

The title compound was prepared as described in Example 166C from Example 269B and azetidine hydrochloride. 1H NMR (300 MHz, CDCl3) δ ppm 1.35 (s, 9H), 1.66 (dd, J=10.9, 2.7 Hz, 4H), 1.84-1.98 (m, 4H), 2.30-2.45 (m, 4H), 2.77 (t, J=6.6 Hz, 1H), 4.36 (t, J=7.6 Hz, 4H), 6.65 (s, 1H), 12.31 (s, 1H); MS (DCI/NH3) m/z 387 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08338623B2
Source datasetuspto-grants-2012_12
ORD IDord-c246b6cbe82a464ea4229312a8b85488
Source noteuspto-grants-2012_12