化工社化工社 化学情報印刷レポート · 研究参考用
Salicyl Alcohol → 2-[(Ethylsulfanyl)methyl]phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Salicyl Alcohol | HCID 5146 | — |
| 反応物 | Ethanethiol | HCID 6343 | — |
| 生成物 | 2-[(Ethylsulfanyl)methyl]phenol | HCID 522167 | 96% |
反応手順
A mixture of 49.6 g (0.4 mol) of 2-hydroxymethyl-phenol and 124 g (2 mol) of ethylmercaptan was heated for 5 hours to 170° C. in a stirred autoclave. Working up as in Example 1 gave 32.2 g (96% of theory) of 2-ethylthiomethyl-phenol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04358616 |
| 出典データセット | uspto-grants-1982_11 |
| ORD ID | ord-eacb17e009e84059b307f1326fc1641a |
| 出典メモ | uspto-grants-1982_11 |