HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicyl Alcohol → 2-[(Ethylsulfanyl)methyl]phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicyl Alcohol | HCID 5146 | — |
| Reactant | Ethanethiol | HCID 6343 | — |
| Product | 2-[(Ethylsulfanyl)methyl]phenol | HCID 522167 | — |
Reaction Steps
49.6 g (0.4 mol) of 2-hydroxymethyl-phenol were reacted with 24.8 g (0.4 mol) of ethylmercaptan in 200 ml of solvent or diluent for 5 hours at 170° C. under autogenous pressure in a VA stirred autoclave. Depending on the solvent or diluent, working up by distillation gave the following yields of 2-ethylthiomethyl-phenol (Table 1):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04358616 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-8198ea50695c4b82826cdebbff718b81 |
| Source note | uspto-grants-1982_11 |