Hydrochloric Acid → HCID 86738632, compound

Participants

Reaction Steps

Ethereal hydrogen chloride was added dropwise to a stirred solution of 2.0 g. of 1-[[2-(2-(4-methylphenyl)ethyl)-1,3-dithiolan-2-yl]methyl]imidazole in 30 ml. of anhydrous ether until precipitation was complete. The product was filtered off, washed with ether, air-dried and recrystallized from methanol/ethyl acetate to yield 1-[[2-(2-(4-methylphenyl)ethyl)-1,3-dithiolan-2-yl]methyl]imidazole hydrochloride--m.p. 206.5°-208° C.

Provenance & Evidence