3-Fluoro-p-anisaldehyde → HCID 13059651, compound

Participants

Reaction Conditions

Reaction Steps

A 7.0 g. amount of N'-(4-amino-2,6-dichlorophenyl)-N,N-dimethylformamidine and 4.6 g. of 3-fluoro-p-anisaldehyde are each dissolved separately in 25 ml. of warm methanol and then combined. The mixture is cooled at 5° C. The crystallized product is collected and washed with ether to provide 8.2 g. of the product of the Example as yellow crystals, m.p. 139°-141° C.

Provenance & Evidence