HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1-(Chloromethyl)-2-iodobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Iodobenzylic alcohol | HCID 107629 | — |
| Product | 1-(Chloromethyl)-2-iodobenzene | HCID 101064 | — |
Reaction Steps
o-Iodobenzyl chloride was prepared from o-iodobenzyl alcohol using thionyl chloride according to the procedure described by Brooks et al, Org. Syn. Coll. Vol. 3, p. 698 (1955). The crude product was distilled at reduced pressure to yield a clear, colorless liquid having a bp of 143°/4 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04360511 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-f48a423008164f6f8117619f5f364853 |
| Source note | uspto-grants-1982_11 |