HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20517475, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 86738636 | HCID 86738636 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20517475 | HCID 20517475 | — |
Reaction Steps
A solution of 1 mg of I-123-o-iodobenzaldehyde prepared in accordance with example 15 in 100 mcl ethanol was placed in a small test tube. One lambda of aniline was added and the mixture allowed to stand for ten minutes. A solution of 2 mg of sodium cyanide in 10 lambda of deionized water was then added and the mixture allowed to stand for an additional ten minutes. Three lambda of acetic acid was then added and the mixture allowed to stand 20 minutes to yield α-anilino-o-iodophenylacetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04360511 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-9cef9f8a8a9d4bd58e45f2dc6ef2ad11 |
| Source note | uspto-grants-1982_11 |