HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 70548183, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 54152323 | HCID 54152323 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70548183 | HCID 70548183 | — |
Reaction Steps
19 g (75 mmols) of 2-acetyl-4-oxo-3-phenyl-pentanoic acid ethyl ester were heated to the boil together with 3.75 g (75 mmols) of hydrazine hydrate in 100 ml of ethanol under nitrogen for 10 hours. The solvent was then distilled off in vacuo and the residue was recrystallised from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04360520 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-50c0483c435c43ca93078dee2c751a8d |
| Source note | uspto-grants-1982_11 |