HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 20517724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 20517720 | HCID 20517720 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20517724 | HCID 20517724 | — |
Reaction Steps
A mixture of 5.3 g 2-fluoro-N-(2-hydroxyphenyl)-N-(1-methyl-piperidin-4-yl)benzamide, 1.1 g of a 55% sodium hydride/oil dispersion and 80 ml dimethylformamide are stirred at 80° for 18 hours. The reaction mixture is worked up as in Example 1(b) to give the heading compound, m.p. 173°-174.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04360525 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-f4f5702f876b400f96de93293bd74f38 |
| Source note | uspto-grants-1982_11 |