HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-(Trifluoromethyl)phenyl)piperazine → 5-Bromo-1-(1-methylethyl)-2-[2-[4-(3-trifluoromethylphenyl)-1-piperazinyl]ethyl]-1H-naphth[1,2-d]imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-(Trifluoromethyl)phenyl)piperazine | HCID 4296 | — |
| Reactant | HCID 20452290 | HCID 20452290 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-Bromo-1-(1-methylethyl)-2-[2-[4-(3-trifluoromethylphenyl)-1-piperazinyl]ethyl]-1H-naphth[1,2-d]imidazole | HCID 13806188 | — |
Reaction Steps
The compound of the title is prepared by condensing 5-bromo-2-(2-chloroethyl)-1-(1-methylethyl)-1H-naphth[1,2-d]imidazole hydrochloride with 1-(3-trifluoromethylphenyl)piperazine. M.p. 161°-62° C. (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04360674 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-24d52891c2bf4f1cb89bf700bfee8125 |
| Source note | uspto-grants-1982_11 |