HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichloroaniline → HCID 178431801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichloroaniline | HCID 12281 | — |
| Reactant | 1,5-Dimethyl-3-oxabicyclo[3.2.0]heptane-2,4-dione | HCID 12356369 | — |
| Product | HCID 178431801 | HCID 178431801 | 34% |
Reaction Steps
7.7 g (0.05 mol) of 1,2-dimethylcyclobutane-1,2-dicarboxylic acid anhydride with 8.1 (0.05 mol) of 3,5-dichloroaniline are heated for 8 hours at 180° C. After cooling, the crude product is recrystallised from ethyl acetate to obtain 5.1 g (34% of theory) of 1,2-dimethylcyclobutane-1,2-dicarboxylic acid-(3,5-dichlorophenyl)-imide, the properties of which are identical to those of the compound produced according to Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04361576 |
| Source dataset | uspto-grants-1982_11 |
| ORD ID | ord-cb9bc12a84524652b1e37eb74e8a3513 |
| Source note | uspto-grants-1982_11 |