Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | L-(+)-Cysteine | HCID 5862 | — |
| Reactant | Ethylene Oxide | HCID 6354 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 53800139 | HCID 53800139 | — |
Reaction Steps
109 g (0.9 mol) of L-cysteine was added into a 2000 ml round-bottomed flask, dissolved with 1000 ml of distilled water, cooled to 10° C. in ice bath, and neutralized to PH˜7 with 24 ml of 1M NaOH solution. 100 ml of ethylene oxide which was pre-cooled was taken at 10° C. and added to the above mixture, the mixture was reacted for 1 h while keeping the temperature at 10° C., then the temperature was raised to room temperature and the reaction was continued for another 1.5 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09359314B2 |
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| Source dataset | uspto-grants-2016_06 |
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| ORD ID | ord-7b964f29635c42e4a24e7344a0e8e296 |
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| Source note | uspto-grants-2016_06 |
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