HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 71542527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 71542528 | HCID 71542528 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 71542527 | HCID 71542527 | 71.6% |
Reaction Steps
(R)-(3-(3-fluoro-4-(6-((1-methyl-1H-tetrazol-5-yl)amino)pyridin-3-yl)phenyl)-2-oxooxazolidin-5-yl)methyl dihydrogen phosphate (140 mg, 0.3 mmol) was dissolved in 15 mL methanol. Sodium methoxide (48 mg, 0.9 mmol) was added, and reacted at room temperature for 12 h. After filtration 110 mg of product was obtained, at a yield of 71.6%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359344B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-9e27ae68c8fa4d8a93516ce804af14b4 |
| Source note | uspto-grants-2016_06 |