HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichlorobenzyl chloride → 6-bromo-1-(2,3-dichlorobenzyl)-3-methyl-1H-indazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichlorobenzyl chloride | HCID 76790 | — |
| Reactant | 1-Benzyl-1H-indole-6-carboxylic acid | HCID 17947875 | — |
| Reactant | HCID 178434209 | HCID 178434209 | — |
| Product | 6-bromo-1-(2,3-dichlorobenzyl)-3-methyl-1H-indazole | HCID 68184280 | 85.5% |
Reaction Steps
The titled compound (228 mg) as a white solid was prepared from the 6-bromo-3-methyl-1H-indazole (152 mg) obtained with the method described in the document (JP 2009-528363 W) and 2,3-dichlorobenzyl chloride (215 mg) according to the method of the process (1) of Example 66.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359350B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-fb2f1b9f1a17469db8243d9fb3caa2ae |
| Source note | uspto-grants-2016_06 |