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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2199990Generated: October 30, 2026

Hydrazine hydrate (1:1) → HCID 178487565, compound

https://huagongshe.com/reaction/2199990

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
Reactant2'-Fluoro-4'-methoxyacetophenoneHCID 592821—
ProductHCID 178487565HCID 178487565—

Reaction Conditions

Temperature140 °C

Reaction Steps

To 2′-fluoro-4′-methoxyacetophenone (5.24 g) was added hydrazine monohydrate (20 mL) at room temperature, and then the reaction mixture was stirred at 140° C. for 20 hours. The precipitated solid was filtered to give the titled compound (4.20 g) as a red solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09359350B2
Source datasetuspto-grants-2016_06
ORD IDord-8640430c58224d3599a5cb7d605701ef
Source noteuspto-grants-2016_06