HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodophenol → 3-(5-Amino-3-methyl-pyrazol-1-yl)-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodophenol | HCID 12272 | — |
| Reactant | HCID 117728990 | HCID 117728990 | — |
| Product | 3-(5-Amino-3-methyl-pyrazol-1-yl)-phenol | HCID 21432439 | — |
Reaction Steps
The title compound was prepared starting from 5-methyl-2H-amino pyrazol (500 mg, 5.1 mmol) and 3-iodo-phenol (1.25 g, 5.7 mmol) by using an analogous procedure to that described for Intermediate A step b. LCMS (Method 3): Rt 0.99 min, m/z=190 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359354B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-2897bb010d7c43e88afe5b40e9b965c2 |
| Source note | uspto-grants-2016_06 |