HRID2200452

反应详情

EQUATION

反应方程式

HRID 2200452 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 4-(4-nitrophenyl)pyridine (274 mg, 1.37 mmol) and Pd—C (10%, 80 mg) in MeOH (10 mL) was hydrogenated under balloon H2 for 20 h. The mixture was then filtered through celite. The filtrate was concentrated in vacuo to give 4-(pyridin-4-yl)aniline as a solid (211 mg).

WORKUP

后处理

  1. filtrationThe mixture was then filtered through celite
  2. concentrationThe filtrate was concentrated in vacuo