HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Methoxyphenyl)-4-methyloxazole → HCID 59679628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Methoxyphenyl)-4-methyloxazole | HCID 68669607 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 59679628 | HCID 59679628 | 95.6% |
Reaction Steps
A solution of 2-(3-methoxyphenyl)-4-methyloxazole (1.1 g, 5.79 mmol) in aqueous hydrogen bromide (10 mL, 48% w/w) was heated to 100° C. for 16 h. The mixture was concentrated to give 3-(4-methyloxazol-2-yl)phenol (0.97 g, crude), which was used without purification. LCMS MH+ 176.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359359B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-ba6771fb9bb042fd8a3a07edbacda34e |
| Source note | uspto-grants-2016_06 |