HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-((3-chloro-4-methoxybenzyl)amino)-2-(methylsulfanyl)pyrimidine-5-carboxylate → HCID 117622625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-((3-chloro-4-methoxybenzyl)amino)-2-(methylsulfanyl)pyrimidine-5-carboxylate | HCID 22025927 | — |
| Reactant | HCID 117622626 | HCID 117622626 | — |
| Product | HCID 117622625 | HCID 117622625 | 54% |
Reaction Steps
The procedures were analogous to Example 1(2). Ethyl 4-((3-chloro-4-methoxybenzyl)amino)-2-(5-azaspiro[2.4]heptan-5-yl)pyrimidine-5-carboxylate (3.4 g, 8.17 mmol) was used in step 2 instead of ethyl 4-((3-chloro-4-methoxybenzyl)amino)-2-(methylthio)pyrimidine-5-carboxylate. Yield: 54%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09359371B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-d8905dcccd924b2293092206cd0909ec |
| Source note | uspto-grants-2016_06 |