HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sebacoyl chloride → 1,10-Decanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sebacoyl chloride | HCID 66072 | — |
| Solvent | Diglyme | HCID 8150 | — |
| Product | 1,10-Decanediol | HCID 37153 | — |
Reaction Steps
In step 2 a di-aldehyde molecule is formed in solution by reacting sebacic acid with thionyl chloride or sulfur oxychloride (SOCl2) to form Sebacoyl chloride. The resultant Sebacoyl chloride is reacted with LiAl[t-OButyl]3H and diglyme to yield 1,10-decanediol as shown below:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09364565B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-92d41ec80059488bb2ef6f458fcea860 |
| Source note | uspto-grants-2016_06 |