Magnesium Hydroxide → N,N,N-Trimethyl-1-adamantylammonium hydroxide

HRID 2201603Notes

Reaction equation

HRID 2201603 reaction equation
C[O:2]C(=O)[O-].[C:6]12([N+:16]([CH3:19])([CH3:18])[CH3:17])[CH2:15][CH:10]3[CH2:11][CH:12]([CH2:14][CH:8]([CH2:9]3)[CH2:7]1)[CH2:13]2.[OH-].[Ca+2].[OH-].[OH-].[Mg+2].[OH-]>O>[OH-:2].[C:6]12([N+:16]([CH3:19])([CH3:18])[CH3:17])[CH2:13][CH:12]3[CH2:11][CH:10]([CH2:9][CH:8]([CH2:14]3)[CH2:7]1)[CH2:15]2

Participants

5

Reactant 3

HCID 73981Magnesium HydroxideHCID 6093208Calcium HydroxideHCID 67399232HCID 67399232, compound

Product 1

HCID 14475644N,N,N-Trimethyl-1-adamantylammonium hydroxide

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The method of the invention comprises reacting 1-adamantyldimethylamine with dimethyl carbonate to produce 1-adamantyltrimethylammonium methylcarbonate. The 1-adamantyltrimethylammonium methylcarbonate is then reacted with calcium hydroxide or magnesium hydroxide in the presence of water to produce 1-adamantyltrimethylammonium hydroxide

Sources & evidence

ORD record
ord-908f212e123943a0b99e7a0db6aaff97
Source dataset
uspto-grants-2016_06
Patent number
US09365490B2

Reaction notes

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