HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 15064526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Ethyl bromodifluoroacetate | HCID 69585 | — |
| Product | HCID 15064526 | HCID 15064526 | — |
Reaction Steps
Et2NH (7.9 g, 108 mmol) was added to ethyl bromodifluoroacetate (20.1 g, 99 mmol) at 30° C. The mixture was stirred for 60 min; then all volatiles were removed under reduced pressure. To the residue was added another 7.9 g of Et2NH and the mixture was stirred another 60 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365495B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-c4c3c09fe5dd4afe88b184f3905ccc2e |
| Source note | uspto-grants-2016_06 |