HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 78320394, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 118558210 | HCID 118558210 | — |
| Product | HCID 78320394 | HCID 78320394 | — |
Reaction Steps
To (S)-tert-butyl 2-(3-(4′-(2-((R)-2-methylpyrrolidin-1-yl)ethyl)biphenyl-4-yl)propanamido)propanoate 2,2,2-trifluoroacetate (4.4 mg, 7.60 mol) was added 4M hydrogen chloride in dioxane (0.665 mL, 2.66 mmol). The reaction was stirred at room temperature for 4 h. The mixture was concentrated to give the title compound. LCMS m/z=409.4 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365511B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-4e71db130e9446aaa54e534bb4ad43a9 |
| Source note | uspto-grants-2016_06 |