HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11194923, compound → HCID 86671522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11194923 | HCID 11194923 | — |
| Reactant | HCID 86671523 | HCID 86671523 | — |
| Product | HCID 86671522 | HCID 86671522 | — |
Reaction Steps
The title compound was prepared from 7b by the general procedure described for compound 9a. Brownish oil (68%). 1H NMR (300 MHz, CDCl3) δ ppm 5.81 (d, J=3.74, 1H), 3.77 (s, 3H), 2.51 (dd, J=3.67, 3.67 Hz, 1H), 2.39 (ddd, J=3.71, 8.76, 12.47 Hz, 1H), 2.03-2.13 (m, 1H), 1.65 (ddd, J=3.68, 9.18, 12.65 Hz, 1H), 1.24 (ddd, J=3.72, 9.18, 12.64 Hz, 1H), 1.11 (s, 3H), 0.97 (s, 3H). Exact mass calculated for C12H15F3O5S m/e 328.06. found 328.44.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365534B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-cbd6de00e55d424ba1dd14f9910972cf |
| Source note | uspto-grants-2016_06 |