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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 220257Generated: October 30, 2026

Acetonitrile → HCID 55023518, compound

https://huagongshe.com/reaction/220257

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetonitrileHCID 6342—
Reactant61381-04-2HCID 840694—
CatalystRhodiumHCID 23948—
SolventMethanolHCID 887—
ProductHCID 55023518HCID 55023518—

Reaction Steps

To a solution of 0.43 g of 2-(3,4-diethoxy-phenyl)-ethylamine in 3 mL MeOH were added 270 mg of 5 wt % Rh/C and 0.22 mL of MeCN. The reaction mixture was stirred under a H2 atmosphere (balloon) for 3 days and then filtrated over a pad of celite and washed with 100 mL MeOH. Concentration in vacuo afforded 0.4 g of [2-(3,4-diethoxy-phenyl)-ethyl]-ethyl-amine as yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08202885B2
Source datasetuspto-grants-2012_06
ORD IDord-4201bcdd52af4248abc2684e4a74e334
Source noteuspto-grants-2012_06