HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminopyridine → HCID 1704483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminopyridine | HCID 10009 | — |
| Reactant | 2-Cyano-3,3-bis(methylthio)acrylamide | HCID 2747746 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 1704483 | HCID 1704483 | — |
Reaction Steps
Dissolved 2-cyano-3,3-bis(methylthio)acrylamide I-2 (1.0 g) in EtOH (15 mL), and heated to 75° C. until solids dissolved. 3-Aminopyridine (1.0 eq., 0.608 g) was then added and solution continued stirring for 2 days. Precipitate formed which was found to be product. Reaction was cooled to room temperature and filtered to obtain 2-((methylthio)(pyridin-3-ylamino)methylene)malononitrile as a yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365556B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-8295c97876384293a17730fa514a6405 |
| Source note | uspto-grants-2016_06 |