HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 58118759, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | 4-(Bromomethyl)oxane | HCID 2773286 | — |
| Product | HCID 58118759 | HCID 58118759 | — |
Reaction Steps
4-(Bromomethyl)tetrahydro-2H-pyran (0.50 g, 2.8 mmol) was dissolved in dimethylamine (40% in water, 5 mL) and the reaction mixture was stirred at RT for 18 hours. The mixture was saturated with NaCl and extracted into Et2O (2×). The combined organic extract was dried (K2CO3), filtered and concentrated in vacuo to give the title compound as a colourless oil (0.40 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365577B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-31a203dfaad54712b97ad6c3733e9c4a |
| Source note | uspto-grants-2016_06 |