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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2203396Generated: October 31, 2026

Dimethylamine → HCID 58118759, compound

https://huagongshe.com/reaction/2203396

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamineHCID 674—
ReactantSodium ChlorideHCID 5234—
Reactant4-(Bromomethyl)oxaneHCID 2773286—
ProductHCID 58118759HCID 58118759—

Reaction Steps

4-(Bromomethyl)tetrahydro-2H-pyran (0.50 g, 2.8 mmol) was dissolved in dimethylamine (40% in water, 5 mL) and the reaction mixture was stirred at RT for 18 hours. The mixture was saturated with NaCl and extracted into Et2O (2×). The combined organic extract was dried (K2CO3), filtered and concentrated in vacuo to give the title compound as a colourless oil (0.40 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09365577B2
Source datasetuspto-grants-2016_06
ORD IDord-31a203dfaad54712b97ad6c3733e9c4a
Source noteuspto-grants-2016_06