HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 8-bromooctanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 8-Bromooctanoic acid | HCID 548275 | — |
| Product | Methyl 8-bromooctanoate | HCID 11107373 | — |
Reaction Steps
Under N2 atmosphere, 8-bromooctanoic acid was dissolved in dry methanol. Concentrated H2SO4 was added drop-wise and the reaction mixture was stirred under reflux for three hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365610B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-321cae9194d44168ab17a7db2f9c927d |
| Source note | uspto-grants-2016_06 |