HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-chloro-1-methyl-5-nitropyridin-2(1H)-one → 3-Amino-5-chloro-1-methylpyridin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-chloro-1-methyl-5-nitropyridin-2(1H)-one | HCID 86703106 | — |
| Reactant | 5-Chloro-1-methyl-3-nitropyridin-2-one | HCID 86703119 | — |
| Product | 3-Amino-5-chloro-1-methylpyridin-2(1H)-one | HCID 86703118 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure for Step E5, but 5-chloro-1-methyl-3-nitro-1H-pyridin-2-one (Step L5) was used instead of 3-chloro-1-methyl-5-nitro-1H-pyridin-2-one to afford the title compound as a gray solid. ESI-MS: tR=0.54 min, [M+H]+ 159/161 (LC-MS 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365576B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-ab0fbb5ee20a458590582f8fc50e8f30 |
| Source note | uspto-grants-2016_06 |