HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86703250, compound → HCID 86703249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86703250 | HCID 86703250 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 86703249 | HCID 86703249 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 240.2 but using 2-(((5-chloro-1-methyl-6-oxo-1,6-dihydropyridin-3-yl)amino)(4-chlorophenyl)methyl)-1-cyclopropyl-1H-pyrrole-3-carboxylic acid (Step 243.3) and stirring the reaction mixture for 2 hr. tR: 0.99 min (LC-MS 6); ESI-MS: 414.1 [M+H]+ (LC-MS 6); TLC (CH2Cl2/MeOH 95:5): Rf=0.32.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09365576B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-915be8d483d74cc3bdd8eabafb644de4 |
| Source note | uspto-grants-2016_06 |