Hydrochloric Acid → HCID 66611962, compound

Participants

Reaction Steps

To a solution of phenylmethyl 4-[(dimethylamino)carbonyl]-5-(1-methyl-1H-pyrazol-4-yl)-2-[(phenylmethyl)oxy]benzoate (may be prepared as described in Description 40; 195 mg, 0.42 mmol) in tetrahydrofuran (4 ml) was added lithium hydroxide (34 mg, 1.42 mmol) and water (1 ml). The mixture was for 18 hours then 2M hydrochloric acid (0.73 ml, 1.45 mmol) was added. The solvent removed in vacuo to give the title compound as a gum. 154 mg.

Provenance & Evidence