HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydro-1,4-benzodioxin-6-carbaldehyde → (2Z)-3-(2,3-dihydro-1,4-benzodioxin-6-yl)-2-{4-[(8-hydroxyoctyl)oxy]phenyl}prop-2-enenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydro-1,4-benzodioxin-6-carbaldehyde | HCID 248127 | — |
| Reactant | HCID 71272497 | HCID 71272497 | — |
| Product | (2Z)-3-(2,3-dihydro-1,4-benzodioxin-6-yl)-2-{4-[(8-hydroxyoctyl)oxy]phenyl}prop-2-enenitrile | HCID 71272407 | 41% |
Reaction Steps
(2Z)-3-(2,3-dihydro-1,4-benzodioxin-6-yl)-2-{4-[(8-hydroxyoctyl)oxy]phenyl}prop-2-enenitrile is prepared starting from {4-[(8-hydroxyoctyl)oxy]phenyl}acetonitrile and commercial 1,4-Benzodioxan-6-carboxaldehyde according the same procedure following for example 1 in 41% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09366906B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-4078e22122f64832af8949f379747059 |
| Source note | uspto-grants-2016_06 |