HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-(Methylenedioxy)phenylacetonitrile → HCID 71272006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-(Methylenedioxy)phenylacetonitrile | HCID 78178 | — |
| Reactant | HCID 59839085 | HCID 59839085 | — |
| Product | HCID 71272006 | HCID 71272006 | 99% |
Reaction Steps
(2Z)-2-(1,3-benzodioxol-5-yl)-3-{4-[(8-hydroxyoctyl)oxy]-3-methoxyphenyl}prop-2-enenitrile is prepared starting from 4-[(8-hydroxyoctyl)oxy]-3-methoxybenzaldehyde and 1,3-benzodioxol-5-ylacetonitrile according the same procedure following for example 10 in 99% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09366906B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-3a0378c08eb54465aa8fd2031525f303 |
| Source note | uspto-grants-2016_06 |