HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-(Methylenedioxy)phenylacetonitrile → (2Z)-2-(1,3-benzodioxol-5-yl)-3-{4-[(6-hydroxyhexyl)oxy]-3-methoxyphenyl}prop-2-enenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-(Methylenedioxy)phenylacetonitrile | HCID 78178 | — |
| Reactant | 4-[(6-Hydroxyhexyl)oxy]-3-methoxybenzaldehyde | HCID 18008791 | — |
| Product | (2Z)-2-(1,3-benzodioxol-5-yl)-3-{4-[(6-hydroxyhexyl)oxy]-3-methoxyphenyl}prop-2-enenitrile | HCID 71272599 | 85% |
Reaction Steps
(2Z)-2-(1,3-benzodioxol-5-yl)-3-{4-[(6-hydroxyhexyl)oxy]-3-methoxyphenyl}prop-2-enenitrile is prepared from 4-[(6-hydroxyhexyl)oxy]-3-methoxybenzaldehyde and 1,3-benzodioxol-5-ylacetonitrile according the same procedure following for example 10 in 85% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09366906B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-e02c8f1c847a4396bf4abc2666424691 |
| Source note | uspto-grants-2016_06 |