HRID2204918

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID78178

3,4-(Methylenedioxy)phenylacetonitrile

C9H7NO2

HCID18008791

未命名化合物

PRODUCTS

生成物

$结构：COc1cc(/C=C(\C#N)c2ccc3c(c2)OCO3)ccc1OCCCCCCO$

HCID71272599

未命名化合物

收率 85%

PROCEDURE

实验过程

(2Z)-2-(1,3-benzodioxol-5-yl)-3-{4-[(6-hydroxyhexyl)oxy]-3-methoxyphenyl}prop-2-enenitrile is prepared from 4-[(6-hydroxyhexyl)oxy]-3-methoxybenzaldehyde and 1,3-benzodioxol-5-ylacetonitrile according the same procedure following for example 10 in 85% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.