反应详情

To a solution of benzyl 6-(tert-butoxycarbonylamino)hexanoate (1 eq) in DCM (0.17 M) was added 4M HCl in dioxane (30 eq). The resulting mixture was stirred at room temperature for 1 hour. The mixture was concentrated en vaccuo. The crude material was dissolved in DCM and precipitated in diethyl ether to give the product as a white solid.

1. concentrationThe mixture was concentrated en vaccuo
2. dissolutionThe crude material was dissolved in DCM
3. customprecipitated in diethyl ether