HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyraldehyde → HCID 78098441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyraldehyde | HCID 6561 | — |
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | HCID 87467929 | HCID 87467929 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 78098441 | HCID 78098441 | 697.2% |
Reaction Steps
Following the general procedure as described in Example 1, 1-(prop-1-en-2-yl)cyclohex-3-enecarbaldehyde (1.50 g, 10 mmol), isobutyraldehyde (0.86 g, 12 mmol) and boron trifluoride etherate (0.14 g, 1.0 mmol) in 1,2-dichloroethane (10 mL) were reacted to give the title product as a colorless liquid (1.55 g, 70% yield). Mixture of E/Z isomers in a ratio 2:1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371262B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-6aba24a65c494bf49423e20bbe10efda |
| Source note | uspto-grants-2016_06 |