HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 78098442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | 1-Ethenyl-3-cyclohexene-1-carboxaldehyde | HCID 89525526 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 78098442 | HCID 78098442 | 399.5% |
Reaction Steps
Following the general procedure as described in Example 1, 1-vinylcyclohex-3-enecarbaldehyde (1.50 g, 10 mmol), acetaldehyde (0.53 g, 12 mmol) and boron trifluoride etherate (0.14 g, 1.0 mmol) in 1,2-dichloroethane (10 mL) were reacted to give the title product as a colorless liquid (0.72 g, 40% yield). Mixture of E/Z isomers in a ratio 1:1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371262B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-03828a84941e4483a3119fd715b88554 |
| Source note | uspto-grants-2016_06 |