HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 89525575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | Ethanone, 1-(4,7,7-trimethylbicyclo[4.1.0]hept-4-en-3-yl)- | HCID 44079 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 89525575 | HCID 89525575 | 818.6% |
Reaction Steps
Following the general procedure as described in Example 1, 1-(4,7,7-trimethylbicyclo[4.1.0]hept-4-en-3-yl)ethanone (1.78 g, 10 mmol), acetaldehyde (0.53 g, 12 mmol) and boron trifluoride etherate (0.14 g, 1.0 mmol) in 1,2-dichloroethane (10 mL) were reacted to give the title product as a colorless liquid (1.82 g, 82% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371262B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-387d9fbbe9ec448e910210f045ce9721 |
| Source note | uspto-grants-2016_06 |