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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2205254Generated: October 26, 2026

Tin tetrachloride → HCID 89525684, compound

https://huagongshe.com/reaction/2205254

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTin tetrachlorideHCID 24287—
Reactantacetaldehyde O-ethyl oximeHCID 533741—
ReactantCyclohexanone, 2-(1-methylethenyl)-HCID 11018939—
Solvent1,2-DichloroethaneHCID 11—
ProductHCID 89525684HCID 8952568480%

Reaction Steps

Following the general procedure as described in Example 17, 2-(prop-1-en-2-yl)cyclohexanone (0.88 g, 6.38 mmol), acetaldehyde O-ethyl oxime (0.67 g, 7.65 mmol), and SnCl4 (1.66 g, 6.38 mmol) in 1,2-dichloroethane (65 ml) were reacted to give the title product as a colorless liquid (1.14 g, 80% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09371262B2
Source datasetuspto-grants-2016_06
ORD IDord-87abdc2c5c5941f78a5085e178a62adb
Source noteuspto-grants-2016_06