HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tin tetrachloride → HCID 131735810, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tin tetrachloride | HCID 24287 | — |
| Reactant | 2,3,4,5-Tetrahydropyridine | HCID 68161 | — |
| Reactant | Cyclohexanone, 2-(1-methylethenyl)- | HCID 11018939 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 131735810 | HCID 131735810 | 69% |
Reaction Steps
Following the general procedure as described in Example 17, 2-(prop-1-en-2-yl)cyclohexanone (0.88 g, 6.38 mmol), 2,3,4,5-tetrahydropyridine (0.64 g, 7.65 mmol), and SnCl4 (1.66 g, 6.38 mmol) in 1,2-dichloroethane (65 ml) were reacted to give the title product as a colorless liquid (0.97 g, 69% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371262B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-d4013b3d13aa4096847e396bcbe5ad89 |
| Source note | uspto-grants-2016_06 |