Potassium Hydroxide → HCID 53241517, compound

Participants

Reaction Steps

In a nitrogen atmosphere, dehydrated toluene (30 ml) and potassium hydroxide (1.8 g, 28.8 mmol) were added to a four-necked flask, and 3-(dimethylamino)-1,2-propanediol (0.57 g, 4.78 mmol) was dropped under agitation. Thereafter, linoleyl methane sulfonate (5.0 g, 14.5 mmol) was added, and refluxing was performed at 110° C. for 3 hours. The reaction was terminated because remaining linoleyl methane sulfonate became 4.8% (degree of conversion: 51.1%, integrated value of isomer: 0.142).

Provenance & Evidence