HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methyl-3-nitrobenzenesulfonyl chloride → N-[5-chloro-2-(methylthio)phenyl]-4-methyl-3-nitrobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methyl-3-nitrobenzenesulfonyl chloride | HCID 560638 | — |
| Reactant | 5-Chloro-2-(methylthio)aniline | HCID 2794577 | — |
| Product | N-[5-chloro-2-(methylthio)phenyl]-4-methyl-3-nitrobenzenesulfonamide | HCID 57378643 | 61% |
Reaction Steps
Following General Procedure B, the title compound (197 mg, 61%) was prepared from 5-Chloro-2-methylsulfanyl-phenylamine (150 mg, 0.87 mmol) and 4-Methyl-3-nitro-benzenesulfonyl chloride (235 mg, 0.87 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371278B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-7cc7734085dc4fbbb126b32709dda097 |
| Source note | uspto-grants-2016_06 |