Acetic Acid → HCID 90036302, compound

Participants

Reaction Conditions

Reaction Steps

tert-Butyl 2-(2-methoxyquinoline-3-carbonyl)hydrazinecarboxylate (1.23 g, 3.87 mmol) was dissolved in DCM (10 mL) and cooled to 0° C. Trifluoroacetic acetic acid (10 mL) was added and the mixture was stirred at room temperature for 1 h. Solvents were evaporated and the residue was washed with water. The product was used without purification in the next step. MS (ES) C11H11N3O2 requires: 217.22, found: 218.

Provenance & Evidence