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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2206079Generated: October 31, 2026

Water → HCID 117988134, compound

https://huagongshe.com/reaction/2206079

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantHCID 117988445HCID 117988445—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 117988134HCID 117988134135.6%

Reaction Steps

To a solution of 4-(3-(cyclopent-1-en-1-yl)-7-methoxy-1H-pyrazolo[3,4-c]pyridin-1-yl)benzenesulfonamide (22 mg) in methanol (10 mL) was added 10% palladium/carbon (6.32 mg) containing water, and the mixture was stirred overnight under hydrogen atmosphere at room temperature. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (30 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09371320B2
Source datasetuspto-grants-2016_06
ORD IDord-50da4e9def294638ab9aa1bf3b7e26c5
Source noteuspto-grants-2016_06