HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131735844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 103563890 | HCID 103563890 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131735844 | HCID 131735844 | — |
Reaction Steps
A mixture of tert-butyl 2-(2,2-dimethylcyclopentyl)hydrazinecarboxylate (2.4 g) and hydrogen chloride in saturated methanol solution (30 mL) was stirred overnight at room temperature. The reaction mixture was concentrated under reduced pressure, and the obtained solid was washed with diethyl ether to give the title compound (2.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371320B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-d3d1321d37be44d6bd66202e71b43523 |
| Source note | uspto-grants-2016_06 |