Hydrochloric Acid → HCID 131735844, compound

HRID 2206254Notes

Reaction equation

HRID 2206254 reaction equation
[CH3:1][C:2]1([CH3:16])[CH2:6][CH2:5][CH2:4][CH:3]1[NH:7][NH:8]C(OC(C)(C)C)=O.[ClH:17]>CO>[ClH:17].[ClH:17].[ClH:17].[CH3:1][C:2]1([CH3:16])[CH2:6][CH2:5][CH2:4][CH:3]1[NH:7][NH2:8]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 103563890HCID 103563890, compound

Product 1

HCID 131735844HCID 131735844, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A mixture of tert-butyl 2-(2,2-dimethylcyclopentyl)hydrazinecarboxylate (2.4 g) and hydrogen chloride in saturated methanol solution (30 mL) was stirred overnight at room temperature. The reaction mixture was concentrated under reduced pressure, and the obtained solid was washed with diethyl ether to give the title compound (2.0 g).

Workup

  1. concentrationThe reaction mixture was concentrated under reduced pressure
  2. washthe obtained solid was washed with diethyl ether

Sources & evidence

ORD record
ord-d3d1321d37be44d6bd66202e71b43523
Source dataset
uspto-grants-2016_06
Patent number
US09371320B2

Reaction notes

Loading…